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Initial stages of metal-organic chemical-vapor deposition of ZrO2 on a FeCrAl alloy
Dalarna University, School of Technology and Business Studies, Material Science.
Dalarna University, School of Technology and Business Studies, Materials Technology.
Dalarna University, School of Technology and Business Studies, Material Science.
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2007 (English)In: Thin Solid Films, ISSN 0040-6090, E-ISSN 1879-2731, Vol. 516, no 6, p. 875-879Article in journal (Refereed) Published
Abstract [en]

The initial stages of metal-organic chemical-vapor deposition of ZrO2 on a model FeCrAl alloy was investigated using synchrotron radiation photoelectron spectroscopy, X-ray absorption spectroscopy, scanning Auger microprobe, and time of flight secondary mass spectrometry. The coatings were grown in ultra-high vacuum at 400 °C and 800 °C using the single source precursor zirconium tetra-tert-butoxide. At 400 °C the coatings mainly consist of tetragonal ZrO2 and at 800 °C amixed ZrO2/Al2O3 layer is formed. The Almetal diffuses from the FeCrAl bulk to themetal/coating interface at 400 °C and to the surface of the coating at 800 °C. The result indicates that the reactionmechanism of the growth process is different at the two investigated temperatures.

Place, publisher, year, edition, pages
Amsterdam: Elsevier , 2007. Vol. 516, no 6, p. 875-879
Keywords [en]
Metal-organic chemical-vapor deposition (MOCVD); Zirconium tetra-tert-butoxide (ZTB); Zirconium oxide; FeCrAl-alloy; Time of flight secondary ionmass spectrometry (ToF-SIMS); X-ray photoelectron spectroscopy (XPS); X-ray absorption spectroscopy (XAS)
National Category
Materials Engineering
Identifiers
URN: urn:nbn:se:du-2961DOI: 10.1016/j.tsf.2007.04.048ISI: 000252980400001OAI: oai:dalea.du.se:2961DiVA, id: diva2:519880
Available from: 2007-10-18 Created: 2007-10-18 Last updated: 2017-12-07Bibliographically approved

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CiteExportLink to record
Permanent link

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Citation style
  • apa
  • ieee
  • modern-language-association-8th-edition
  • vancouver
  • chicago-author-date
  • chicago-note-bibliography
  • Other style
More styles
Language
  • de-DE
  • en-GB
  • en-US
  • fi-FI
  • nn-NO
  • nn-NB
  • sv-SE
  • Other locale
More languages
Output format
  • html
  • text
  • asciidoc
  • rtf