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  • 1.
    Gyhlesten Back, Jessica
    et al.
    Dalarna University, School of Technology and Business Studies, Materials Technology.
    Surreddi, Kumar Babu
    Dalarna University, School of Technology and Business Studies, Materials Technology.
    Microstructure analysis of martensitic low alloy carbon steel samples subjected to deformation dilatometry2019In: Materials Characterization, ISSN 1044-5803, E-ISSN 1873-4189, Vol. 157, article id 109926Article in journal (Refereed)
  • 2. Habainy, J.
    et al.
    Iyengar, S.
    Surreddi, Kumar Babu
    Dalarna University, School of Technology and Business Studies, Materials Technology.
    Lee, Y.
    Dai, Y.
    Formation of oxide layers on tungsten at low oxygen partial pressures2018In: Journal of Nuclear Materials, ISSN 0022-3115, E-ISSN 1873-4820, Vol. 506, no SI, p. 26-34Article in journal (Refereed)
    Abstract [en]

    This work focuses on the oxidation of tungsten in inert gas atmospheres containing oxygen and moisture. It is particularly relevant for the European Spallation Source where the tungsten target is cooled by purified helium gas and the 5 MW proton beam can raise the maximum target temperature beyond the threshold for oxidation. Tungsten discs were oxidized isothermally at 400° to 900 °C for 2 h in pure helium and helium mixed with oxygen and water vapor, with varying partial pressures up to 500 Pa. Tungsten was oxidized even with a small amount of oxygen (≤5 ppm) present in industrially pure helium. Non-isothermal oxidation of tungsten foils was carried out in water vapor (∼100 Pa), in situ in an environmental scanning electron microscope. On specimens oxidized in inert gas containing water vapor (2 h, pH2O" role="presentation" style="box-sizing: border-box; margin: 0px; padding: 0px; display: inline-block; line-height: normal; font-size: 14.4px; word-spacing: normal; word-wrap: normal; white-space: nowrap; float: none; direction: ltr; max-width: none; max-height: none; min-width: 0px; min-height: 0px; border: 0px; position: relative;">pH2O ∼790 Pa), Auger electron spectroscopy studies confirmed the presence of a thin oxide layer (40 nm) at 400 °C. At 500 °C the oxide layer was 10 times thicker. A dark, thin and adherent oxide layer was observed below 600 °C. Above this temperature, the growth rate increased substantially and the oxide layer was greenish, thick and porous. Oxide layers with varying stoichiometry were observed, ranging from WO3 at the surface to WO2 at the metal-oxide interface. For comparison, oxidation of tungsten alloysin He-5%O2 was studied. The implications of this work on the design and operation of the helium loop for cooling the target are discussed.

  • 3. Habainy, J.
    et al.
    Lee, Y.
    Surreddi, Kumar Babu
    Dalarna University, School of Technology and Business Studies, Materials Technology.
    Prosvetov, A.
    Simon, P.
    Iyengar, S.
    Dai, Y.
    Tomut, M.
    Study of heavy ion beam induced damage in tungsten for high power target applications2019In: Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, ISSN 0168-583X, E-ISSN 1872-9584, Vol. 439, p. 7-16Article in journal (Refereed)
    Abstract [en]

    The spallation material at ESS is pure tungsten, which is cooled by gaseous helium flow. To study the behaviour of tungsten under dynamic beam conditions at ESS, pure tungsten specimens have been irradiated at the M3-beamline of the UNILAC facility at GSI Helmholtz Centre for Heavy Ion Research. Tungsten specimens of two thicknesses, 26 μm and 3 mm, were exposed to pulsed uranium and gold ion beams for fluences up to 7.5 · 1013 ions·cm−2 at 4.8 MeV/nucleon. Nanoindentation tests were performed on the cross section of the irradiated 3 mm sample, and microhardness was measured on the top surface. The measured data are compared with the calculated damage values, and a correlation between the radiation induced damage and the observed mechanical property is presented. Thermal diffusivities of foil samples irradiated up to four different fluences were measured with a Laser Flash Apparatus (LFA). The observed changes in the mechanical and thermal properties of irradiated tungsten were used to estimate the changes of operational temperature and mechanical stresses in the ESS target material with the progress of radiation damage, using coupled thermal and mechanical simulations. From the pulsed beam induced dynamic oscillations of thin tungsten specimens, information on fatigue properties of tungsten under irradiation was drawn. In addition to pure tungsten, oxidised tungsten samples were irradiated. This is to investigate the stability of the adhesive oxide layer under pulsed beam conditions, which would be formed due to oxygen impurities in the helium cooling loop. The irradiated oxide scale was examined using Auger Electron Spectroscopy (AES) and Scanning Electron Microscopy (SEM). 

  • 4.
    Olsson, Mikael
    et al.
    Dalarna University, School of Technology and Business Studies, Materials Technology.
    Surreddi, Kumar Babu
    Dalarna University, School of Technology and Business Studies, Materials Technology.
    Scratch testing of cemented carbides - Influence of Co binder phase and WC grain size on surface deformation and degradation mechanisms2018In: Proceedings of The 18th Nordic Symposium on Tribology - Nordtrib 2018 / [ed] Staffan Jacobson, Uppsala: Uppsala University, 2018Conference paper (Refereed)
    Abstract [en]

    In the present study, the microstructural response of some commercial cemented carbide grades during scratchinghas been analyzed and evaluated by a number of post-test characterization techniques. The influence of Co binder phase content and WC grain size on the deformation and degradation on a WC grain size scale and on a composite scaleare evaluated. The results clearly illustrate the complexity of deformation, degradation and wear of cemented carbide and the dynamics of the diamond stylus / cemented carbide contact during the scratching event. For all cementedcarbide grades the microstructure has a strong impact on the observed degradation mechanisms and the resistance to deformation and degradation was found to increase with decreasing Co content and decreasing WC grain size.

  • 5.
    Olsson, Mikael
    et al.
    Dalarna University, School of Technology and Business Studies, Materials Technology.
    Surreddi, Kumar Babu
    Dalarna University, School of Technology and Business Studies, Materials Technology.
    Thin hard CVD and PVD coatings and their potential in steel wire drawing applications2018In: Proceedings of The 18th Nordic Symposium on Tribology - NORDTRIB 2018 / [ed] Staffan Jacobson, Uppsala: Uppsala University, 2018Conference paper (Refereed)
    Abstract [en]

    In the present work, the potential of using thin hard CVD and PVD coatings in order to improve the performance of cemented carbide steel wire drawing nibs is evaluated. Coating materials include some state-of-the-art CVD and PVD coatings and pre- and post-coating treatments were used to improve the surface topography of the coated functional surfaces. The tribological performance of the coatings has been evaluated by sliding wear tests and wire drawing experiments under well controlled conditions. Post-test characterization of the coated nibs using 3D optical surface profilometry, scanning electron microscopy and energy dispersive X-ray spectroscopy illustrates the pros and cons of the two deposition techniques but also that the coatings have a potential to improve the performance of cemented carbide nibs in steel wire drawing applications.

  • 6. Scudino, S.
    et al.
    Surreddi, Kumar Babu
    Dalarna University, School of Technology and Business Studies, Materials Technology.
    Shear band morphology and fracture behavior of cold-rolled Zr52.5Ti5Cu18Ni14.5Al10 bulk metallic glass under tensile loading2017In: Journal of Alloys and Compounds, ISSN 0925-8388, E-ISSN 1873-4669, Vol. 708, p. 722-727Article in journal (Refereed)
    Abstract [en]

    The effect of the shear bands generated by cold rolling on the tensile ductility and fracture behavior of the Zr52.5Ti5Cu18Ni14.5Al10 bulk metallic glass (BMG) is analyzed. The results reveal significant changes in the fracture behavior of the cold-rolled material with respect to the as-cast BMG. Fracture in the cold-rolled glass occurs along the pre-existing shear bands forming an angle of 45° with the loading direction. In addition, the fracture morphology shows a regular vein pattern oriented along the shear direction, which indicates that a considerable shear stress is active on the fracture plane. This is in contrast to the fracture behavior of the as-cast glass, where the normal stress plays a significant role. Here, the fracture angle is 55° and the fracture surface is characterized by the conventional irregular pattern of radiating ridges. Finally, work-hardening was observed in the cold-rolled BMG even in the absence of visible shear band intersection. Possible alternative mechanisms for determining this behavior are discussed. © 2017 Elsevier B.V.

  • 7.
    Scudino, S.
    et al.
    IFW Dresden, Inst Complex Mat, Solidificat Proc & Complex Struct, Helmholtzstr 20, D-01069 Dresden, Germany..
    Surreddi, Kumar Babu
    Dalarna University, School of Technology and Business Studies, Materials Technology.
    Wang, G.
    Shanghai Univ, Lab Microstruct, Shanghai 200444, Peoples R China..
    Liu, G.
    Xi An Jiao Tong Univ, State Key Lab Mech Behav Mat, Xian 710049, Peoples R China.;Xi An Jiao Tong Univ, Sch Mat Sci & Engn, Xian 710049, Peoples R China..
    Effect of stress concentration on plastic deformation of Zr41.2Ti13.8Cu12.5Ni10Be22.5 bulk metallic glass under compressive loading2016In: Materials letters (General ed.), ISSN 0167-577X, E-ISSN 1873-4979, Vol. 179, p. 202-205Article in journal (Refereed)
    Abstract [en]

    The influence of different sources of stress concentration on the plastic deformation of the Zr41.2Ti13.8Cu12.5Ni10Be22.5 metallic glass during room temperature compression tests is evaluated. Stress concentration introduced by sample geometry has a significant effect on the mechanical properties: in contrast to the specimen with square cross-section, which shows negligible plastic deformation, a substantial improvement in the plasticity can be achieved for the sample with round cross-section. Simulations of the stress distribution during the compression tests reveal that the stress concentration at the interface corners is responsible for the early fracture of the sample with square cross-section. Additionally, stress concentration during compression tests in the samples with square cross-section can be significantly reduced, and plastic deformation can be enhanced, by removing the interface corners as well as by reducing the friction arising between loading platens and specimen. 

  • 8.
    Surreddi, Kumar Babu
    et al.
    Dalarna University, School of Technology and Business Studies, Materials Technology.
    Oikonomou, C.
    Uddeholms AB, SE-68385 Hagfors, Sweden..
    Karlsson, P.
    Orebro Univ, Dept Mech Engn, SE-70182 Orebro, Sweden..
    Olsson, Mikael
    Dalarna University, School of Technology and Business Studies, Materials Technology.
    Pejryd, L.
    Orebro Univ, Dept Mech Engn, SE-70182 Orebro, Sweden..
    In-situ micro-tensile testing of additive manufactured maraging steels in the SEM: Influence of build orientation, thickness and roughness on the resulting mechanical properties2018In: La Metallurgia Italiana, ISSN 0026-0843, no 3, p. 27-33Article in journal (Refereed)
    Abstract [en]

    Selective laser melting (SLM) is frequently used additive manufacturing technique capable of producing various complex parts including thin-wall sections. However the surface roughness is a limiting factor in thin sections produced by SLM process when strength is the main criterion. In this study, the influence of build orientation, thickness and roughness on the resulting mechanical properties of as-built test samples was investigated. Various thin sheets of EN 1.2709 maraging steel built in horizontal and vertical orientations produced by SLM were investigated using in-situ micro-tensile testing in a scanning electron microscope. The mechanical strength and deformation mechanisms were analyzed and explained based on thickness and build orientation. Increased ductility was observed in thicker samples as well as in the horizontal build samples. The results illustrate the potential of the in-situ test technique and aspects important to consider in design guidelines for thin AM structures.

  • 9.
    Surreddi, Kumar Babu
    et al.
    Dalarna University, School of Technology and Business Studies, Materials Technology.
    Oikonomou, Christos
    Karlsson, Patrik
    Olsson, Mikael
    Dalarna University, School of Technology and Business Studies, Materials Technology.
    Pejryd, Lars
    In-situ Micro-tensile Testing of Additive Manufactured Maraging Steels in the SEM: Influence of Build Orientation, Thickness and Roughness on the Resulting Mechanical Properties2017In: Proceedings Euro PM 2017: International Powder Metallurgy Congress and Exhibition2017: Session 30: Mechanical Behaviour of AM Materials, 2017, article id Session 30Conference paper (Refereed)
    Abstract [en]

    Selective laser melting (SLM) is frequently used additive manufacturing technique capable of producing various complex parts including thin-wall sections. However the surface roughness is a limiting factor in thin sections produced by SLM process when strength is the main criterion. In this study, the influence of build orientation, thickness and roughness on the resulting mechanical properties of as-built test samples was investigated. Various thin sheets of EN 1.2709 maraging steel built in horizontal and vertical orientations produced by SLM were investigated using in-situ micro-tensile testing in a scanning electron microscope. The mechanical strength and deformation mechanisms were analyzed and explained based on thickness and build orientation. Increased ductility was observed in thicker samples as well as in the horizontal build samples. The results illustrate the potential of the in-situ test technique and aspects important to consider in design guidelines for thin AM structures.

  • 10.
    Surreddi, Kumar Babu
    et al.
    Dalarna University, School of Technology and Business Studies, Materials Technology.
    Olsson, Mikael
    Dalarna University, School of Technology and Business Studies, Materials Technology.
    Wear of cemented carbide nibs in steel wire drawing2018In: The 18th Nordic Symposium on Tribology – NORDTRIB 2018 / [ed] Prof. Staffan Jacobson, 2018Conference paper (Other academic)
    Abstract [en]

    The tribological interaction between a cemented carbide drawing die and a steel wire under lubricated wire drawing conditions has been characterized using 3D optical surface profilometry, scanning electron microscopy and energy dispersive X-ray spectroscopy. The results show that wear of the cemented carbides mainly is located to three different wear zones, i) at the entrance of the reduction zone, ii) at the exit of the reduction zone/ entrance of the bearing zone and iii) at the exit of the bearing zone. In the first wear zone, wear of the cemented carbide occurs on a WC grain size level and is controlled by plastic deformation, cracking and fragmentation of individual WC grains. In the second wear zone, wear of the cemented carbide is controlled by chipping of small WC/Co composite fragments resulting in craters, ~ 10μm in diameter.

  • 11.
    Surreddi, Kumar Babu
    et al.
    Dalarna University, School of Technology and Business Studies, Materials Technology.
    Yvell, Karin
    Dalarna University, School of Technology and Business Studies, Materials Technology.
    Norgren, Susanne
    Sandvik Mining and Rock Technology, Rock Tools division, Sweden; Department of Engineering Sciences, Uppsala University, Sweden.
    Olsson, Mikael
    Dalarna University, School of Technology and Business Studies, Materials Technology.
    Characterization of surface degradation and wear damage Of cemented carbide in rock drilling2018In: The 18th Nordic Symposium on Tribology – NORDTRIB 2018 / [ed] Prof. Staffan Jacobson, 2018Conference paper (Other academic)
    Abstract [en]

    In this work, worn top hammer drill bit buttons after underground drifting in Granodiorite are analysed using scanning electron microscopy (SEM), Auger electron spectroscopy (AES) and electron backscatter diffraction (EBSD) to understand the dominant surface failure and wear mechanisms on the flank wear land region, i.e. the outer side of the gauge row cemented carbide buttons. SEM shows that the worn surface of the flank wear land is partly covered with islands of a thin rock material transfer layer and that the exposed cemented carbide show deformed, cracked and fragmented WC grains. AES gives that the transferred rock material is mainly located on the surface but may penetrate into cemented carbide microstructure to a depth of 1-2 WC grain diameters. Finally, EBSD reveals that the deformation of the cemented carbide in the flank wear land region is located to a thin zone, about ~10 μm in depth.

  • 12. Vattur Sundaram, M.
    et al.
    Surreddi, Kumar Babu
    Dalarna University, School of Technology and Business Studies, Materials Technology.
    Hryha, E.
    Veiga, A.
    Berg, S.
    Castro, F.
    Nyborg, L.
    Enhanced densification of PM steels by liquid phase sintering with boron-containing master alloy2017In: Metallurgical and Materials Transactions. A, ISSN 1073-5623, E-ISSN 1543-1940, Vol. 49A, no 1, p. 255-263Article in journal (Refereed)
    Abstract [en]

    Reaching high density in PM steels is important for high-performance applications. In this study, liquid phase sintering of PM steels by adding gas-atomized Ni-Mn-B master alloy was investigated for enhancing the density levels of Fe- and Mo- prealloyed steel powder compacts. The results indicated that liquid formation occurs in two stages, beginning with the master alloy melting (LP-1) below and eutectic phase formation (LP-2) above 1373 K (1100 °C). Mo and C addition revealed a significant influence on the LP-2 temperatures and hence on the final densification behavior and mechanical properties. Microstructural embrittlement occurs with the formation of continuous boride networks along the grain boundaries, and its severity increases with carbon addition, especially for 2.5 wt pct of master alloy content. Sintering behavior, along with liquid generation, microstructural characteristics, and mechanical testing revealed that the reduced master alloy content from 2.5 to 1.5 wt pct (reaching overall boron content from 0.2 to 0.12 wt pct) was necessary for obtaining good ductility with better mechanical properties. Sintering with Ni-Mn-B master alloy enables the sintering activation by liquid phase formation in two stages to attain high density in PM steels suitable for high-performance applications. © 2017 The Author(s)

  • 13.
    Vattur Sundaram, Maheswaran
    et al.
    Chalmers University of Technology.
    Surreddi, Kumar Babu
    Dalarna University, School of Technology and Business Studies, Materials Technology.
    Hryha, Eduard
    Chalmers University of Technology.
    Veiga, Angela
    CEIT, Pº Manuel Lardizábal 15, 20018 San Sebastián, Spain.
    Berg, Siguard
    Höganäs AB, SE-263 83 Höganäs, Sweden.
    Castro, Francisco
    CEIT, Pº Manuel Lardizábal 15, 20018 San Sebastián, Spain.
    Nyborg, Lars
    Chalmers University of Technology.
    Full Densification in PM Steels Through Liquid Phase Sintering and HIP Approach2018In: Euro PM2018 Proceedings, 2018Conference paper (Refereed)
    Abstract [en]

    High-density powder metallurgy (PM) components are required for high-performance applications. Liquid phase sintering (LPS) is one such method to improve the densification, especially the master alloy route is preferred due to the flexibility in tailoring the alloying contents. In this study, gas atomised Ni-Mn-B master alloy powder of size fraction < 45 µm was admixed with water atomised iron and Mo-prealloyed powder. During sintering, there was a significant densification due to LPS where the liquid formation occurred in two stages, one from the master alloy melting and another from the eutectic liquid formation, enabling densities > 95%. The microstructural investigation revealed that the surface densification was achieved after sintering in H2 containing atmosphere. Capsule free hot isostatic pressing was performed on these samples to achieve full density. This approach of combining LPS and capsule free hot isostatic pressing demonstrates the potential in reaching full densification in high-performance PM steel components.

  • 14. Wang, Z.
    et al.
    Prashanth, K. G.
    Surreddi, Kumar Babu
    Dalarna University, School of Technology and Business Studies, Materials Technology.
    Suryanarayana, C.
    Eckert, J.
    Scudino, S.
    Pressure-assisted sintering of Al–Gd–Ni–Co amorphous alloy powders2018In: Materialia, ISSN 2589-1529, Vol. 2, p. 157-166Article in journal (Refereed)
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